Study on Shock-induced Phase Transition of CsPbBr3 through Pulsed Discharge of Cylindrical Wire Array in Water Medium

doi:10.12382/bgxb.2024.0276

Abstract

Abstract:

Perovskite is regarded as one potential material for next-generation photovoltaic devices owing to its outstanding photoelectric characteristics which can be easily adjusted by phase transitions.However,the technology for intercepting and preparing the metastable perovskites is still in its infancy.The impact loading method has a significant advantage of high quenching rate,and enables the capture of metastable phases and facilitating their subsequent recovery and preparation.To achieve the impact phase transition treatment of CsPbBr₃,the cylindrical converging shockwaves are generated by the pulsed discharge of cylindrical wire array in water medium for studying the shock-induced phase transition of CsPbBr₃.The delicate control of shock pressure is applied to act on CsPbBr₃ powder by adjusting the charging voltage.After experiments,the samples are recovered and characterized.The characterized results reveale that the shock waves generated by pulsed discharge can induce phase transition in CsPbBr₃ powder under appropriate shock pressures (above 2 GPa).Additionally,the typical phenomena such as grain refinement,lattice distortion and nano-defects are observed in the recovered samples after shock-wave treatment.This study demonstrates that pulsed discharge of cylindrical wire array in water medium is a feasible converging shock wave loading technique,providing a novel approach to shock-induced phase transition loading.

Key words: perovskite, pulsed discharge, shockwave, convergent effect, impact phase transition

CLC Number:

TB39

ZHANG Xueying, GAO Xin, XIAO Zeqi, LIU Kaiyuan, YUE Lidan, QIN Zhiqi, CHEN Pengwan. Study on Shock-induced Phase Transition of CsPbBr₃ through Pulsed Discharge of Cylindrical Wire Array in Water Medium[J]. Acta Armamentarii, 2025, 46(2): 240276-.

Figures/Tables 16

References 49

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序号	K
1	2.16
2	8.65
3	13.52
4	13.52

序号	K
1	2.16
2	8.65
3	13.52
4	13.52

序号	峰值电流/kA	周期/μs	脉宽/μs
1	320.09	164.04	43.09
2	451.12	186.74	50.87
3	633.85	160.06	46.05
4	631.17	160.06	45.49

序号	峰值电流/kA	周期/μs	脉宽/μs
1	320.09	164.04	43.09
2	451.12	186.74	50.87
3	633.85	160.06	46.05
4	631.17	160.06	45.49

序号	W_t/(J·m^-1)	τ/μs	T/μs	p_m/MPa	p_r/MPa	p_N/MPa
1	56250	21.53	41	189.26	151.39	586.34
2	225000	25.44	44.5	334.39	267.49	1035.98
3	351562.5	23.03	40	463.38	370.67	1435.58

Study on Shock-induced Phase Transition of CsPbBr₃ through Pulsed Discharge of Cylindrical Wire Array in Water Medium

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Figures/Tables 16

References 49

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序号	N	U₀/kV	E/kJ	前驱体
1	15	6	4.50	CsPbBr₃
2	15	12	18.00	CsPbBr₃
3	15	15	28.13	CsPbBr₃
4	15	15	28.13

原料和样品	A峰			B峰			C峰			D峰(主峰)			E峰			F峰
原料和样品	峰位/ (°)	相对峰强	偏差	峰位/ (°)	相对峰强	偏差	峰位/ (°)	相对峰强	偏差	峰位/ (°)	相对峰强	偏差	峰位/ (°)	相对峰强	偏差	峰位/ (°)	相对峰强	偏差
原料	15.30	0.26		21.56	0.58		30.46	0.27		30.80	1		37.91	0.45		43.81	0.35
1号样品	15.26	0.26	-0.04	21.56	0.38	0	30.46	0.44	0	30.80	1	0	37.91	0.18	0	43.80	0.24	-0.01
2号样品	15.34	0.20	0.04	21.68	1.16	0.12	30.62	0.72	0.16	30.91	1	0.11	37.91	0.71	0	44.01	0.72	0.20
3号样品	15.36	0.15	0.06	21.69	0.76	0.13	30.62	0.82	0.16	30.91	1	0.11	37.91	0.91	0	43.94	1.08	0.13

原料和样品	晶型	a	b	c	α/ (°)	β/ (°)	γ/ (°)
原料	四方	5.87721	5.87721	23.23167	90	90	90
1号样品	四方	5.83567	5.83568	31.49033	90	90	90
2号样品	单斜	8.23600	5.79100	5.80800	90	134.799	90
3号样品	单斜	8.70096	4.09157	6.19904	90	110.20	90

原料	1号样品	2号样品	3号样品
5.786	5.802	5.764	5.771
4.118	4.118	4.094	4.103
2.932	2.932	2.917	2.922
2.901	2.901	2.891	2.890
2.371	2.371	2.371	2.371
2.065	2.065	2.059	2.060

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